NMR Spectroscopy

Basic Principles, Concepts, and Applications in Chemistry

Author: Harald Günther

Publisher: Wiley

ISBN: 9780471952015

Category: Science

Page: 602

View: 5444

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As with its predecessor, this edition uses a practical non-mathematical approach. Features a number of recent developments in the field including two-dimensional methods, solid state NMR and an enlarged treatment of Fourier Transform methods. Contains numerous two-color diagrams.

Ein- und zweidimensionale NMR-Spektroskopie

Eine Einführung

Author: Horst Friebolin

Publisher: John Wiley & Sons

ISBN: 3527334920

Category: Nuclear magnetic resonance spectroscopy

Page: 452

View: 6819

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Diese vollstandig uberarbeitete und aktualisierte Neuauflage des klassischen Lehrbuches beinhaltet neben den Grundlagen der NMR-Spektroskopie auch die der Spektreninterpretation. Ohne viel Mathematik bietet der Text eine Einleitung und deckt somit auch den Lehrstoff von Hochschulkursen ab. Der Hauptanteil des Buches ist nach wie vor der NMR-Spektroskopie an Losungen gewidmet, doch wurden auch verstarkt Untersuchungen an Festkorpern und die Analyse von Biopolymeren berucksichtigt. Zum Schluss werden einige Einsatzmoglichkeiten der Kernspintomographie und der Kombination von Tomographie und Spektroskopie besprochen. Erganzt wurde jedes Kapitel um Aufgaben, deren Losungsvorschlage im Anschluss an Kapitel 14 zu finden sind. Mit seiner ubersichtlichen Darstellung ist dieses Buch ein Muss fur Studenten, Dozenten und Anwender der NMR-Spektroskopie in der Chemie, Biochemie und Pharmazie.

Organische Chemie

Studieren kompakt

Author: Paula Yurkanis Bruice

Publisher: Pearson Deutschland GmbH

ISBN: 3868941029

Category:

Page: 1165

View: 9228

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Ein- und zweidimensionale NMR-Spektroskopie

Eine Einführung

Author: Horst Friebolin

Publisher: John Wiley & Sons

ISBN: 3527334920

Category: Nuclear magnetic resonance spectroscopy

Page: 452

View: 1310

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Diese vollstandig uberarbeitete und aktualisierte Neuauflage des klassischen Lehrbuches beinhaltet neben den Grundlagen der NMR-Spektroskopie auch die der Spektreninterpretation. Ohne viel Mathematik bietet der Text eine Einleitung und deckt somit auch den Lehrstoff von Hochschulkursen ab. Der Hauptanteil des Buches ist nach wie vor der NMR-Spektroskopie an Losungen gewidmet, doch wurden auch verstarkt Untersuchungen an Festkorpern und die Analyse von Biopolymeren berucksichtigt. Zum Schluss werden einige Einsatzmoglichkeiten der Kernspintomographie und der Kombination von Tomographie und Spektroskopie besprochen. Erganzt wurde jedes Kapitel um Aufgaben, deren Losungsvorschlage im Anschluss an Kapitel 14 zu finden sind. Mit seiner ubersichtlichen Darstellung ist dieses Buch ein Muss fur Studenten, Dozenten und Anwender der NMR-Spektroskopie in der Chemie, Biochemie und Pharmazie.

NMR Spectroscopy in Liquids and Solids

Author: Vladimir I. Bakhmutov

Publisher: CRC Press

ISBN: 148226272X

Category: Medical

Page: 360

View: 7703

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NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics. The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR— including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.

NMR in Biological Systems

From Molecules to Human

Author: K.V.R. Chary,Girjesh Govil

Publisher: Springer Science & Business Media

ISBN: 1402066791

Category: Science

Page: 524

View: 1460

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During teaching NMR to students and researchers, we felt the need for a text-book which can cover modern trends in the application of NMR to biological systems. This book covers the entire area of NMR in Biological Sciences (Biomolecules, cells and tissues, animals, plants and drug design). As well as being useful to researchers, this is an excellent book for teaching a course on NMR in Biological Systems.

NMR spectroscopy

modern spectral analysis

Author: Ursula Weber,Herbert Thiele

Publisher: Vch Verlagsgesellschaft Mbh

ISBN: 9783527288281

Category: Science

Page: 393

View: 902

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The state-of-the-art in NMR spectral analysis. This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters. Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WIN-DYNAMICS, and direct data exchange between all these programs is possible. Readers are shown how they can obtain maximum structural information from their 1 D NMR spectra with time-saving computer assistance. Practical problems that can occur and their solutions are discussed at length using clear, easy-to-follow examples. Both homo- and heteronuclear and first- and second-order spin systems are demonstrated. Moreover, relaxation analysis, nuclear Overhauser effects and magnetic site exchange are all covered in this hands-on guide to NMR spectral analysis.

Structure Elucidation by Modern NMR

A Workbook

Author: Helmut Duddeck,Wolfgang Dietrich,Gabor Toth

Publisher: Steinkopff

ISBN: N.A

Category: Science

Page: 211

View: 9186

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During the last few years, routine applications of NMR (Nuclear Magnetic Resonance) techniques have developed at a tremendous pace. The latest generation of spectrometers have enabled chemists to perform new types of experiments, such as spinlock and inverse-detected methods. This third, revised and expanded edition introduces the latest methodologies and incorporates them into new exercises.

NMR Spectroscopy Explained

Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology

Author: Neil E. Jacobsen

Publisher: John Wiley & Sons

ISBN: 9780470173343

Category: Science

Page: 640

View: 4609

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NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.

Ullmann's Encyclopedia of Industrial Chemistry

Author: Wiley-VCH

Publisher: Wiley-VCH

ISBN: 9783527303854

Category: Science

Page: 30080

View: 2159

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89 years of expertise in applied and industrial chemistry - Ullmann's is back in print! Generations of chemists and engineers have relied on the well structured and trusted information from Ullmann's Encyclopedia - and you still can count on Ullmann's with the current 6th edition in print. Ullmann's is a synonym for the world's most current and trustworthy knowledge in everything that relates to the chemical industry, be it processes, chemicals, products, analytical chemistry, pharmaceuticals, biotechnology..........you name it, Ullmann's has it - well over 800 articles on over 30 000 printed pages in 40 volumes. Organized in alphabetical order, the chapters are easy to read and excellent starting points to introduce you to any topic. Over 15 000 tables and 25 000 figures (some of them in color) make it easy for you to quickly find what you are looking for. Countless literature and patent references guide you to the relevant and accessible primary literature. Numerous cross-references point you to relevant chapters in the same context and a well organized index volume enables searching for keywords. Finding what you need is very simple indeed and you won't have to ask for a user's manual for this massive work! Supervised by an internationally acclaimed advisory board, the articles are written by over 3000 international experts from industry and universities, thoroughly edited to uniform style and layout in an in-house office. All figures are re-drawn to give a maximum of clarity and uniformity in style. Compared to the prior edition, almost 60% of the material has either been newly written or thoroughly updated. The rest has been checked for validity and newer references have been added throughout.

CARBOHYDRATE CHEMISTRY. Edition en anglais

Author: Geert-Jan Boons

Publisher: Blackie Academic & Professional

ISBN: N.A

Category: Medical

Page: 508

View: 2347

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The chemistry and biochemistry of carbohydrates have become key research areas throughout the world. Responding to the enormous interest expressed in these fields, this new book has brought together a range of contributors, each working at the forefront of carbohydrate chemistry and biochemistry to provide concise authoritative and timely review of these exciting areas. Aimed at chemists, biochemists and biologists, the reader will find this book an invaluable introduction to and review of the most important developments in carbohydrate chemistry. As a distinct chemical group, the carbohydrates comprising mono-, oligo-, and polysaccharides and their derivatives are the most abundant group of natural products. From simple monosaccharides produced in photosynthesis to polysaccharides built in complex biochemical reactions, carbohydrates are produced in huge quantities by plant and animal life. Apart from dietary and structural uses in plants and animals, it is now well established that carbohydrates play a number of key roles in living systems. From cell-cell recognition to hormonal activities, carbohydrates are implicated in a wide range of cellular processes. This new understanding has forced the study of carbohydrates to the forefront of modern chemical research. For example, the nature of the role of carbohydrates in living systems offers the potential to provide important lead compounds in the development of new bioactive molecules. Similarly, the relative abundance of carbohydrates is prompting research aimed at utilizing simple monosaccharides as starting materials for a range of high value chemical product, offering a renewable alternative to current starting materials.

The student's lab companion

laboratory techniques for organic chemistry : standard scale and microscale

Author: John W. Lehman

Publisher: Pearson College Div

ISBN: N.A

Category: Science

Page: 388

View: 5945

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This comprehensive lab companion provides a thorough introduction to all of the significant operations used in the organic lab, for both traditional-scale and microscale applications. It includes enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. lab.Makes substantive revisions of many operations to clarify existing material and add new information. Emphasizes environmentally friendly (i.e. green ) lab experiments. Adds a new section on Chemistry and the Environment.A useful guide for chemists and other professionals who do laboratory work in the scientific fields.

Operational Organic Chemistry

A Problem-solving Approach to the Laboratory Course

Author: John W. Lehman

Publisher: Prentice Hall

ISBN: 9780136000921

Category: Science

Page: 897

View: 6656

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This comprehensive laboratory text provides a thorough introduction to all of the significant operations used in the organic lab and includes a large selection of traditional-scale experiments and minilabs. Its unique problem-solving approach encourages students to think in the laboratory by solving a scientific problem in the process of carrying out each experiment. The Fourth Edition contains a new introductory section, "Chemistry and the Environment," which includes a discussion of the principles of green chemistry. Several green experiments have been added, and some experiments from the previous editions have been revised to make them greener.

Encyclopedia of Environmental Analysis and Remediation

Author: Robert A. Meyers

Publisher: Wiley-Interscience

ISBN: 9780471166399

Category: Science

Page: 675

View: 500

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With the growing concern over the environment, new industries and research areas have been developed to identify, monitor, regulate, and legislate environmental interactions as well as to determine and repair existing environmental damage. For both the expert and the newcomer, a quick, convenient, and comprehensive source is needed to answer questions on the rapidly increasing amount of environmental information. The Encyclopedia of Environmental Analysis and Remediation (EEAR) responds to this need by providing the reader with an in-depth examination of the environmental analysis and remediation fields in a single eight-volume reference source.

Nuclear Magnetic Resonance Spectroscopy

An Introduction to Principles, Applications, and Experimental Methods

Author: Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge

Publisher: Wiley

ISBN: 1119295238

Category: Science

Page: 480

View: 5479

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Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Microscale Operational Organic Chemistry

A Problem-solving Approach to the Laboratory Course

Author: John W. Lehman

Publisher: Prentice Hall

ISBN: N.A

Category: Science

Page: 844

View: 5135

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This practical guide to the core operations in the organic lab gives an excellent selection of clever microscale experiments, enabling users to have an excellent resource that encourages scientific problem-solving. The unique problem-solving approach given in this guide encourages readers to master major lab operations, explaining why they are carried out the way they are. Readers will understand each scientific problem, formulate a meaningful hypothesis, and then solve the problem. Sections on qualitative organic analysis and basic operations such as glassware use, conducting chemical reactions, washing and drying operations, purification operations, measuring, and instrumental analyses round out this handy reference work. The extensive appendices, bibliography, and basic operations sections make this an excellent desktop resource for organic chemists and other lab technicians.

High Resolution NMR

Theory and Chemical Applications

Author: Edwin D. Becker

Publisher: Elsevier

ISBN: 9780080508061

Category: Science

Page: 424

View: 9489

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High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate" level, with mathematics used to augment, rather than replace, clear verbal descriptions of the phenomena. The book is intended to allow a graduate student, advanced undergraduate, or researcher to understand NMR at a fundamental level, and to see illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The presentation is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. Likewise, no previous background in NMR is assumed, since the book begins with a description of the basic physics, together with a brief account of the historical development of the field. This third edition of High Resolution NMR preserves the "conversational" approach of the previous editions that has been well accepted as a teaching tool. However, more than half the material is new, and the remainder has been revised extensively. Problems are included to reinforce concepts in the book. Uses mathematics to augment, not replace, verbal explanations Written in a clear and conversational style Follows the successful format and approach of two previous editions Revised and updated extensively--about 70 percent of the text is new Includes problems and references to additional reading at the end of each chapter

Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry

Author: L. M. Jackman,S. Sternhell

Publisher: Elsevier

ISBN: 1483280942

Category: Science

Page: 474

View: 3907

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Application of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry, Second Edition covers the theoretical background necessary for the intelligent application of NMR spectroscopy to common problems encountered in organic chemistry. This book is composed of five parts, and begins with introduction to the theory and practice of nuclear magnetic resonance. The succeeding chapter deals with the theory of chemical effects in NMR spectroscopy. These topics are followed by a discussion on the application of chemical shift to organic compound analysis and the principles of the spin-spin coupling .The final chapter considers the applications of time- dependent phenomena in NMR spectroscopy. This book will prove useful to analytical chemists and researchers in the allied fields.